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We report the first simultaneous lidar observations of thermosphere‐ionosphere sporadic nickel and Na (TISNi and TISNa) layers in altitudes ∼105–120 km over Yanqing (40.42°N, 116.02°E), Beijing. From two years of data spanning April 2019 to April 2020 and July 2020 to June 2021, TISNi layers in May and June possess high densities with a maximum of 818 cm⁻³on 17 May 2021, exceeding the density of main layer peak (∼85 km) by ∼4 times. They correlate with strong sporadic E layers observed nearby. TISNa layers occur at similar altitudes as TISNi with spatial‐temporal correlation coefficients of ∼1. The enrichment of Ni in TISNi is evident as the [TISNi]/[TISNa] column abundance ratios are ∼1, about 10 times the main layer [Ni]/[Na] ratios. These results are largely explained by neutralization of converged Ni⁺and Na⁺ions via recombination with electrons. Calculations show direct recombination dominating over dissociative recombination above ∼105 km.

We report the first simultaneous, common‐volume lidar observations of thermosphere‐ionosphere Fe (TIFe) and Na (TINa) layers in Antarctica. We also report the observational discovery of nearly one‐to‐one correspondence between TIFe and aurora activity, enhanced ionization layers, and converging electric fields. Distinctive TIFe layers have a peak density of ~384 cm⁻³and the TIFe mixing ratio peaks around 123 km, ~5 times the mesospheric layer maximum. All evidence shows that Fe⁺ion‐neutralization is the major formation mechanism of TIFe layers. The TINa mixing ratio often exhibits a broad peak at TIFe altitudes, providing evidence for in situ production via Na⁺neutralization. However, the tenuous TINa layers persist long beyond TIFe disappearance and reveal gravity wave perturbations, suggesting a dynamic background of neutral Na, but not Fe, above 110 km. The striking differences between distinct TIFe and diffuse TINa suggest differential transport between Fe and Na, possibly due to mass separation.